Welcome to the Center for Crystallographic Research. Formed in July of 2007, to support the research endeavors at Michigan State University, with resources for Single Crystal X-ray Diffraction (SCXRD), Powder X-ray Diffraction (PWXRD). The Faculty has acquired instrumentation from various sources which include Bruker and a Rigaku SCXRD instruments, a Bruker PWXRD. Please check out the links and information within these pages and I hope that they provide a useful tool to discover the great advantages that X-ray diffraction can have on the research performed here at
Michigan State University and surrounding academic institutions.
2021 the CENTER ADDED HIGH PRESSURE CRYSTALLOGRAPHIC TECHNIQUES TO ITS LIST OF RESEARCH OPTIONS.
Analytical services provided using x-ray diffraction. Single Crystal, Powder Diffraction and High Pressure Crystallography.
NEWS
January 9, 2025
Publication in conjunction with University of Idaho
Our 2025 JMCA article has been selected by the Royal Society of Chemistry for inclusion in the Top 50 Most Popular Articles of 2025, based on citations, downloads, and reader engagement. Announcment. The successful determination of the crystal structure of compound 5 using electron diffraction from a powder sample clearly strengthened the manuscript.
Publication in conjunction with University of Idaho.
How Far Can Trinitromethyl Substitution Be Pushed on a Single 1,2,3-Triazole Ring?
J. Singh, H. Gao, R.J. Staples, J.E. Burch, J.M. Shreeve Org. Letts. , 2025, XX, ASAP.
Publication in conjunction with University of Idaho.
High performance and insensitive energetic compounds from the intelligent assembly of nitramino/gem-nitromethyl group and oxadiazoles.
F. Chen, Q. Yu, Z. Guo, K. Peng, W. Zhou, W. Yi, R.J. Staples, J.M. Shreeve Mater. Adv., 2025, 6, 9203-9208.
Publication in conjunction with University of Idaho.
A base-assisted one-pot cyclization and potassium association route to a very thermally stable bistetrazole salt
P. Saini, J. Singh, R.J. Staples, J.M. Shreeve J. Mater. Chem. A, 2025, 13, 37427-37434.
Publication in conjunction with University of Idaho.
Dancing with the Performance of 2-(Nitrooxy)ethan-1-aminium Nitrate (NOEAN): A Green Energetic Oxidizer for Solid Rocket Propulsion.
S. Lal, R.J. Staples, J.M. Shreeve Organic Letters, 2025, 27(43), 12183-12187.
Publication in conjunction with Michigan State University.
A Neutral Dy(II) Bis(Amide): Synthesis, Magnetism, and a P4(2-) Complex.
R. Jena, F. Benner, R.J. Staples, S. Demir, A.L. Odom Inorg. Chem. 2025, 64(41), 20643-20651.
Publication in conjunction with Washington University, St. Louis.
Macrocycle Side Chain Crowding Enables Tunable Curvature from Planar to Wrinkled and Wavy Hydrogen-Bond Sheets.
J.R. Pathan, X. Pang, S.C. Olsen, A.M. Abarna, R.J. Staples, J. Samanta, V.B. Birman, C. Ke JACS A, 2025, 147(32), 28570-28576.
Strategic integration of nitroimino and dinitromethyl explophores onto tetrazole: K2DNMNAT as a material with enhanced thermal stability and optimized oxygen balance.
P. Saini, J. Singh, R.J. Staples, J.M. Shreeve J. Mater. Chem. A, 2025, 13, 17421-17428.
Publication in conjunction with University of Idaho.
Strategies for balancing safety in oxadiazole tetrazole derivatives: the role of the oxime group.
P. Saini, J. Singh, V. Thaltiri, R.J. Staples, J.M. Shreeve J. Mater. Chem. A, 2025, 6, 3338-3343.
Publication in conjunction with University of Idaho.
Coordination-driven safer and sustainable energetic materials.
J. Singh, R.J. Staples, J.M. Shreeve J. Materials Chemistry A , 2025, 13(16), 11475-485.
Publication in conjunction with University of Idaho.
Isomer-driven pyrazole Frameworks: structural and zwitterionic insights for advanced energetics.
V. Thaltiri, R.J. Staples, J. Burch, A. Bera, S.R. Vennapusa, J.M. Shreeve J. Materials Chemistry A , 2025, 13(13) 9394-9401.
Publication in conjunction with University of Idaho.
Synthesis of insensitive, high-density energetic materials through molecular self-assembly.
J. Zhang, J. Zhang, R.J. Staples, J. Zhang J.M. Shreeve J. Mater. Chem A. , 2025,13, 5164-5168.
Publication in conjunction with University of Idaho.
Tailoring the Energetic Properties of Pyrazole Hybrids Through Functionalization with Dinitromethyl and N-Hydroxytetrazole.
V. Thaltiri, R.J. Staples, J.M. Shreeve Organic Chem., 2024, 89(24), 18612-18618.